Composition Analysis of Iron-Silicate Coagulation Structure with EPMA
نویسندگان
چکیده
منابع مشابه
Importance of Carbon Contamination in High-Resolution (FEG) EPMA of Silicate Minerals.
The effect of carbon contamination on the analysis of carbon-coated silicate minerals at 5 kV for X-ray energies 0.7-4 keV is examined. For individual spot analyses, carbon is found to deposit adjacent to the beam spot forming ring-shaped deposits with no impact on the analysis. Carbon contamination becomes important for closely spaced analyses such as multipoint transects, where each subsequen...
متن کاملHYDROTHERMAL SYNTHESIS AND CHARACTERIZATION OF VANADIUM SILICATE MOLECULAR SIEVES WITH ANALCIME, MAGEDIITE AND ZSM-11 STRUCTURE
Vanadium silicates such as V-Al-analcime, V-analcime, V-magediite and V-ZSM-11 were synthesized using vanadium pentoxide or vanadyl sulfates. Vanadium silicates with analcime structure with and without aluminum (V-Al-analcime, V-analcime) were prepared as pure phase by hydrothermal crystallization from a gel with molar composition of (1 SiO2; 0.2 V2O5; 1 Na2O; 0.034 Al2O3; 35.7 H2O) and (1 SiO2...
متن کاملQuantitative TEM analysis of a hexagonal mesoporous silicate structure.
TEM analysis of mesoporous materials is generally undertaken to give qualitative results. Accurate quantitative analysis is demonstrated in this study. A systematic image analysis of a powder form of a hexagonal mesoporous material known as KIT-6 is conducted using a transmission electron microscope (TEM). Three types of image contrast typically appear in this material (a hexagonal honeycomb st...
متن کاملStructure, composition, and defect control during plasma spray deposition of ytterbium silicate coatings
Environmental barrier coatings (EBCs) are needed to protect SiC structures exposed to high temperatures in water vapor-rich environments. Recent studies of a tri-layer EBC system consisting of a silicon layer attached to the SiC, a mullite diffusion barrier and a lowsteam volatility ytterbium silicate topcoat have shown some promise for use at temperatures up to 1316 C. However, the performance...
متن کاملSEM and EPMA analysis of un-usual hydride structure in in-pile cracked Zircaloy-cladding
The hydride distribution in a cracked Zircaloy cladding tube has been investigated by neutron radiography, Scanning Electron Microscopy (SEM) and Hydrogen measurements. The crack occurred during handling in the spent fuel pool. Back Scattered Electron images showed some unexpected contrasts in zones with high hydrogen concentrations near cracks. This phase has been studied by SEM and EPMA. Afte...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of the Japan Institute of Metals and Materials
سال: 1988
ISSN: 0021-4876,1880-6880
DOI: 10.2320/jinstmet1952.52.12_1221